G. Mobus et Bj. Inkson, Three-dimensional reconstruction of buried nanoparticles by element-sensitive tomography based on inelastically scattered electrons, APPL PHYS L, 79(9), 2001, pp. 1369-1371
Energy-filtered transmission electron microscopy is used to image the nanoc
omposite FeAl+Y2O3, an oxide-dispersion-strengthened intermetallic alloy, o
ver a tilt range of +/- 60 degrees using inelastically scattered electrons
only. The properties of electron spectroscopic imaging are exploited to rec
over a projection relationship between the three-dimensional chemical conce
ntration distribution and the micrographs. This allows recovery of the full
information on volume shape, distribution, and homogeneity of the buried n
anoparticles by backprojection. Restrictions to low atomic number, common i
n bio-objects, are here overcome at the expense of higher electron exposure
s. (C) 2001 American Institute of Physics.