Surface gratings associated with holographic volume gratings in photorefrac
tive crystals of iron-doped lithium niobate have been studied using diffrac
tion of a reflected probe beam and high-resolution phase-shifted interferom
etric profilometry. Both techniques show that the surface gratings exist in
the form of periodical corrugations of the same period as that of the volu
me grating. The maximum amplitude of the periodical surface relief measured
by both techniques is close to 6.5 nm. We also demonstrated that the perio
dical electric forces on the surface were capable of assembling polystyrene
microspheres along the fringes of the grating. Large amplitude of the peri
odic electric field (1.6x10(4) V/cm) is associated with the photogalvanic e
ffect. (C) 2001 American Institute of Physics.