Preconcentration of trace elements in sea water with 8-hydroxyquinoline immobilized polyacrylonitrile hollow fiber membrane for determination by inductively coupled plasma-mass spectrometry

Citation
B. Wen et al., Preconcentration of trace elements in sea water with 8-hydroxyquinoline immobilized polyacrylonitrile hollow fiber membrane for determination by inductively coupled plasma-mass spectrometry, INT J ENV A, 77(2), 2000, pp. 95-109
Citations number
22
Language
INGLESE
art.tipo
Article
Categorie Soggetti
Environment/Ecology
Journal title
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY
ISSN journal
0306-7319 → ACNP
Volume
77
Issue
2
Year of publication
2000
Pages
95 - 109
Database
ISI
SICI code
0306-7319(2000)77:2<95:POTEIS>2.0.ZU;2-1
Abstract
8-Hydroxyquinoline immobilized on polyacrylonitrile hollow fiber membrane w as synthesized and used for the preconcentration of cadmium, lead, copper, mangenese, bismuth, indium, cobalt, beryllium and silver in sea water prior to their determination by inductively coupled plasma-mass spectrometry. Th e optimum experimental conditions such as pH, sample flow rate and volume o f eluents were investigated. The concentration factor of at least 300 for a nalytes of interest in sea water and separation of matrix components can be achieved. The recommended method has been applied for the determination of trace elements in coastal sea water. The results indicated that the recove ry ranged from 91% to 107%, and the relative standard deviations were found to be less than 5% for trace elements at ng/L level.